2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

Base Information

Chemical Name:2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide
CAS No.:59179-84-9
Molecular Formula:C₃₁H₂₆ClN₃O₅
Molecular Weight:556.018
Hs Code.:

2-benzoyl-4-chloro-N<sup>α</sup>-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

Synonyms:2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

Chemical Property:

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Technology Process of 2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

There total 4 articles about 2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5491-18-9
2-(benzyloxycarbonylamino)-2-phenylacetic acid

: 59179-84-9
2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / hexamethylphosphoric acid triamide / 0.17 h / -5 °C

2: hexamethylphosphoric acid triamide / Ambient temperature

With thionyl chloride; In N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jm00133a006

Reference yield:

: 29176-43-0
<2-Benzoyl-4-chlor-phenyl-carbamoylmethyl>-carbaminsaeure-benzylester

: 59179-84-9
2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 30percent HBr / acetic acid / 1.5 h / Ambient temperature

2: hexamethylphosphoric acid triamide / Ambient temperature

With hydrogen bromide; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid;
DOI:10.1021/jm00133a006

Reference yield:

: 15396-72-2
N--glycin

: 719-59-5
5-chloro-2-aminobenzophenone

: 59179-84-9
2-benzoyl-4-chloro-N^α-(benzyloxycarbonyl)-DL-(α-phenylglycyl)glycinanilide

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, -10 deg C, 20 min, 2.) CH₂Cl₂, a) 0 deg C, 1.25 h, b) RT, 1.5 h, c) reflux, overnight;
DOI:10.1021/jm00181a013