dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester

Base Information

• Chemical Name: dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester
• CAS No.: 858641-30-2
• Molecular Formula: C₁₃H₁₅NO₂Te
• Molecular Weight: 344.868
• Mol file: 858641-30-2.mol

Synonyms:dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester

Chemical Property of dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester

Chemical Property:

Purity/Quality:

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Technology Process of dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester

There total 1 articles about dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

bis(N,N-dimethylcarbamoyl) ditelluride (106011-93-2) + 4-phenyl-3-butyne-2-one (1817-57-8) → dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester (858641-30-2)

Guidance literature:

With sodium tetrahydroborate; In ethanol; N,N-dimethyl-formamide; at -50 - 20 ℃;

DOI:10.1246/bcsj.78.899

Reference yield: 80.0%

dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester (858641-30-2) + 3-aminophenol hydrochloride (51-81-0) → C16H14NOTe(1+)*Cl(1-)

Guidance literature:

In ethanol; for 6h; Reflux;

DOI:10.1021/acs.inorgchem.1c02585

Reference yield: 79.0%

dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester (858641-30-2) → C10H9NOTe (936924-43-5) + 3-Methyl-5-phenyl-isotellurazole (88459-86-3)

Guidance literature:

With hydroxylamine-O-sulfonic acid; In methanol; for 2h; Heating;

DOI:10.1246/bcsj.80.567

upstream raw materials:

bis(N,N-dimethylcarbamoyl) ditelluride

4-phenyl-3-butyne-2-one

Downstream raw materials:

C₁₀H₉NOTe

3-Methyl-5-phenyl-isotellurazole