phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

Base Information

Chemical Name:phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside
CAS No.:1082073-92-4
Molecular Formula:C₁₄H₁₆O₃
Molecular Weight:232.279
Hs Code.:

Synonyms:phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

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Technology Process of phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

There total 4 articles about phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1082073-78-6
(+)-(2S,3S,6R)-2-methyl-6-phenyl-3,6-dihydro-2H-pyran-3-ol

: 108-24-7
acetic anhydride

: 1082073-92-4
phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo8015709

Reference yield: 51.0%

: 66003-76-7
Diphenyliodonium triflate

: 54621-94-2
3,4-di-O-acetyl-L-fucal

: 1082073-92-4
phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; tetrabutyl-ammonium chloride; triethylamine; In N,N-dimethyl-formamide; at 125 ℃; for 48h; stereoselective reaction; Sealed tube;
DOI:10.1039/d0ob00247j

Reference yield: 42.0%

: 98-09-9
benzenesulfonyl chloride

: 54621-94-2
3,4-di-O-acetyl-L-fucal

: 1082073-92-4
phenyl 4-O-acetyl-2,3,6-trideoxy-α-L-threo-hex-2-enopyranoside

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; lithium carbonate; In 1,4-dioxane; at 140 ℃; for 40h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201403195