(trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester

Base Information

Chemical Name:(trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester
CAS No.:244008-55-7
Molecular Formula:C₁₁H₂₄NO₆PS
Molecular Weight:329.354
Hs Code.:

Synonyms:(trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester

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Chemical Property of (trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester

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Technology Process of (trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester

There total 2 articles about (trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 124-63-0
methanesulfonyl chloride

: 244008-52-4
(trans-1,4-cyclohexanolyl)phosphoramidic acid diethyl ester

: 244008-55-7
(trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/jo9904664

Reference yield:

: 27489-62-9
trans-4-hydroxycyclohexylamine

: 244008-55-7
(trans-1,4-cyclohexanol methanesulfonyl)phosphoramidic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine / dimethylformamide / 3.5 h

2: 62 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Substitution / 2: Substitution;
DOI:10.1021/jo9904664