C₃₇H₅₈O₅

Base Information

• Chemical Name: C₃₇H₅₈O₅
• CAS No.: 1350724-55-8
• Molecular Formula: C₃₇H₅₈O₅
• Molecular Weight: 582.865
• Mol file: 1350724-55-8.mol

Synonyms:C₃₇H₅₈O₅

Chemical Property of C₃₇H₅₈O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₅₈O₅

There total 4 articles about C₃₇H₅₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

C22H35BrO3 + 5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene (56469-10-4) → C37H58O5 (1350724-55-8)

Guidance literature:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene; With potassium fluoride; potassium carbonate; In acetone; for 0.5h; Reflux; Inert atmosphere;

C₂₂H₃₅BrO₃; In acetone; for 48h; Reflux; Inert atmosphere;

DOI:10.1021/jm200529h

Reference yield:

1,12-dibromododecane (3344-70-5) → C37H58O5 (1350724-55-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: Reflux; Inert atmosphere

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

With potassium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1021/jm200529h

Reference yield:

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene (60526-81-0) → C37H58O5 (1350724-55-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

With potassium fluoride; boron tribromide; potassium carbonate; In dichloromethane; acetone;

DOI:10.1021/jm200529h

upstream raw materials:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene

1,12-dibromododecane

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

cis-5-hydroxyl-2-phenyl-1,3-dioxane

Downstream raw materials:

2-{12-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]dodecyloxy}propane-1,3-diol