(O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

Base Information

Chemical Name:(O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride
CAS No.:1365255-67-9
Molecular Formula:C₁₂H₁₇ClNO₃PS
Molecular Weight:321.765
Hs Code.:

Synonyms:(O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

Suppliers and Price of (O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

Chemical Property:

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Technology Process of (O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

There total 4 articles about (O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 18961-96-1
O-phenylphosphorodichloridothioate

: 39613-92-8,62062-56-0,62062-65-1
alanine isopropyl ester hydrochloride

: 1365255-67-9
(O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

Guidance literature:: With triethylamine; In dichloromethane; at -70 - 20 ℃; Temperature; Time; Inert atmosphere; Large scale;

Reference yield:

: 18961-96-1
O-phenylphosphorodichloridothioate

: 1454896-03-7
(S)-isopropyl 2-aminopropanoate methanesulfonic acid salt

: 1365255-67-9
(O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 22h;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1365255-67-9
(O-phenyl-N-(S)-1-(isopropoxycarbonyl)eth-1-yl)thiophosphoramidic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorothiophosphine; triethylamine / dichloromethane / -70 - 20 °C / Inert atmosphere; Large scale

2: triethylamine / dichloromethane / -70 - 20 °C / Inert atmosphere; Large scale

With trichlorothiophosphine; triethylamine; In dichloromethane;