tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0)

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Chemical Name:tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0)
CAS No.:121357-56-0
Molecular Formula:C₃₃H₅₆NiO₅P₂Si₂
Molecular Weight:709.613
Hs Code.:

Synonyms:tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0)

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Chemical Property of tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0)

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Technology Process of tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0)

There total 1 articles about tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 107855-82-3,121284-67-1
1,3,5-Tri-tert-butyl-2-{[1-[2,2-dimethyl-1-trimethylsilanyloxy-prop-(E)-ylidenephosphanyl]-1-trimethylsilanyloxy-meth-(Z)-ylidene]-phosphanyl}-benzene

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 121357-56-0
tricarbonyl(η1-4-t-butyl-1-{2,4,6-tri(t-butyl)phenyl}-2,4-bis(trimethylsiloxy)-1,3-diphospha(1,3)butadiene)nickel(0)

Guidance literature:: In diethyl ether; byproducts: CO; under inert gas, ether, 15 min at 0°C; 8 d at 8°C; sepn. of crystals from mother liquor, drying in vacuo.; elem. anal.;
DOI:10.1016/0022-328X(88)80153-0