(E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate

Base Information

• Chemical Name: (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate
• CAS No.: 1256343-76-6
• Molecular Formula: C₃₀H₃₉NO₅
• Molecular Weight: 493.643

Synonyms:(E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate

Chemical Property of (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate

Chemical Property:

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Technology Process of (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate

There total 1 articles about (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

JMC 7-E (1056462-71-5) + 3-isobutyl-5-methylhexanoic acid (1256343-75-5) → (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate (1256343-76-6)

Guidance literature:

With dmap; bis(2-oxo-1,3-oxazolidin-3-yl)phosphinous chloride; triethylamine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1002/cbic.201000343

Reference yield:

1-Bromopentane (110-53-2) + (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate (1256343-76-6) → Br(1-)*C35H50NO5(1+)

Guidance literature:

In acetonitrile; for 12h; Reflux;

DOI:10.1002/cbic.201000343

Reference yield:

C11H23Br (1256343-77-7) + (E)-2-benzyloxymethyl-5-oxo-4-(pyridin-4-ylmethylene)tetrahydrofuran-2-ylmethyl 3-isobutyl-5-methylhexanoate (1256343-76-6) → Br(1-)*C41H62NO5(1+)

Guidance literature:

In acetonitrile; for 12h; Reflux;

DOI:10.1002/cbic.201000343

upstream raw materials:

JMC 7-E

3-isobutyl-5-methylhexanoic acid

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