1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide

Base Information

Chemical Name:1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide
CAS No.:1415396-53-0
Molecular Formula:C₂₀H₁₇N₂O₂*I
Molecular Weight:444.272
Hs Code.:

Synonyms:1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide

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Chemical Property of 1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide

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Technology Process of 1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide

There total 2 articles about 1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1632-83-3
1-Methylbenzimidazole

: 2-bromomethyl-6-phenyl-4-pyrone

: 1415396-53-0
1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide

Guidance literature:: With potassium iodide; In acetonitrile; at 70 ℃; for 10h;
DOI:10.2174/157017812803521153

Reference yield:

: 230617-82-0
4-Hydroxymethyl-6-phenyl-4H-pyran-2-one

: 1415396-53-0
1-methyl-3-[(4-oxo-6-phenyl-4H-pyran-2-yl)methyl]-benzimidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; sulfuric acid / water / 18 h / 70 °C

2: potassium iodide / acetonitrile / 10 h / 70 °C

With sulfuric acid; hydrogen bromide; potassium iodide; In water; acetonitrile;
DOI:10.2174/157017812803521153