N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide

Base Information

• Chemical Name: N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide
• CAS No.: 140367-87-9
• Molecular Formula: C₃₂H₅₀N₂O₄SSi
• Molecular Weight: 586.912

Synonyms:N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide

Chemical Property of N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide

There total 2 articles about N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

Methanesulfonic acid (S)-2-[(4-methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-4-(3-triisopropylsilanyloxy-4,5-dihydro-3H-pyrrol-2-yl)-butyl ester (140368-02-1) → N-(4-Methoxy-benzyl)-4-methyl-N-((1R,6S,8aR)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide (140367-87-9) + N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide (140367-87-9)

Guidance literature:

With sodium tetrahydroborate; potassium carbonate; In ethanol; Heating; 0 deg C to reflux;

DOI:10.1016/0040-4039(91)80195-C

Reference yield: 10.0%

Methanesulfonic acid (S)-2-[(4-methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-4-(3-triisopropylsilanyloxy-4,5-dihydro-3H-pyrrol-2-yl)-butyl ester (140368-02-1) → N-(4-Methoxy-benzyl)-4-methyl-N-((1R,6S,8aR)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide (140367-87-9) + N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide (140367-87-9)

Guidance literature:

With sodium tetrahydroborate; potassium carbonate; In ethanol; Heating; 0 deg C to reflux;

DOI:10.1016/0040-4039(91)80195-C

Reference yield: 68.0%

N-(4-Methoxy-benzyl)-4-methyl-N-((1S,6S,8aS)-1-triisopropylsilanyloxy-octahydro-indolizin-6-yl)-benzenesulfonamide (140367-87-9) → N-((1S,6S,8aS)-1-Hydroxy-octahydro-indolizin-6-yl)-N-(4-methoxy-benzyl)-4-methyl-benzenesulfonamide

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile;

DOI:10.1016/0040-4039(91)80195-C

upstream raw materials:

Methanesulfonic acid (S)-2-[(4-methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-4-(3-triisopropylsilanyloxy-4,5-dihydro-3H-pyrrol-2-yl)-butyl ester

Downstream raw materials:

(1S,6S,8aS)-1-acetoxy-6-aminooctahydroindolizidine

N-((1S,6S,8aS)-1-Hydroxy-octahydro-indolizin-6-yl)-4-methyl-benzenesulfonamide

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