tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

Base Information

Chemical Name:tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane
CAS No.:102583-44-8
Molecular Formula:C₂₀H₃₆OSi
Molecular Weight:320.591
Hs Code.:

Synonyms:tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

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Chemical Property of tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

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Technology Process of tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

There total 7 articles about tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102393-47-5
3,3-Dimethyl-cyclohexanecarbonyl chloride

: 102583-44-8
tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) lithium diisopropylamide / 1.) THF, -78 deg C, 45 min; 2.) THF-HMPA, a.) -78 deg C, 15 min; b.) RT, 3 h

With lithium diisopropyl amide;

Reference yield:

: 19879-92-6
(E/Z)-2-bromo-1-ethenylcyclopropane

: 102583-44-8
tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) lithium diisopropylamide / 1.) THF, -78 deg C, 45 min; 2.) THF-HMPA, a.) -78 deg C, 15 min; b.) RT, 3 h

With lithium diisopropyl amide;

Reference yield:

: 102393-75-9
(3,3-Dimethyl-cyclohexyl)-(2-vinyl-cyclopropyl)-methanone

: 102583-44-8
tert-Butyl-{(3,3-dimethyl-cyclohexyl)-[2-vinyl-cycloprop-(Z)-ylidene]-methoxy}-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butoxide / tetrahydrofuran; 2-methyl-propan-2-ol / 3 h / Ambient temperature

2: 1.) lithium diisopropylamide / 1.) THF, -78 deg C; 2.) THF-HMPA, -78 deg C then RT

With lithium diisopropyl amide; potassium tert-butylate; In tetrahydrofuran; tert-butyl alcohol;