3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

Base Information

Chemical Name:3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt
CAS No.:1311291-40-3
Molecular Formula:C₂HF₃O₂*C₁₆H₁₅FN₂O₄S
Molecular Weight:464.394
Hs Code.:

Synonyms:3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

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Chemical Property of 3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

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Technology Process of 3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

There total 7 articles about 3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: C₂₀H₂₃FN₂O₄S

: 76-05-1
trifluoroacetic acid

: 1311291-40-3
3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

Guidance literature:: at 20 ℃; for 1h;

Reference yield:

: 1311291-37-8
3-(5-hydroxycarbonyl-3-methylthiophen-2-yl)propanoic acid tert-butyl ester

: 1311290-63-7
4-amidino-2-fluorophenol trifluoroacetate

: 1311291-40-3
3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In pyridine; at 20 ℃;

Reference yield:

: 1311291-36-7
(E)-3-(5-benzyloxycarbonyl-3-methylthiophen-2-yl)-2-propenoic acid tert-butyl ester

: 1311291-40-3
3-[5-(4-amidino-2-fluorophenoxycarbonyl)-3-methylthiophen-2-yl]propanoic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In pyridine; ethanol;