1-TERT-BUTYLOXYCARBONYL-4-AMINO-PIPERAZINE

Base Information

• Chemical Name: 1-TERT-BUTYLOXYCARBONYL-4-AMINO-PIPERAZINE
• CAS No.: 118753-66-5
• Molecular Formula: C9H19 N3 O2
• Molecular Weight: 201.269
• Hs Code.: 2933599090
• Mol file: 118753-66-5.mol

Synonyms:1,1-Dimethylethyl4-amino-1-piperazinecarboxylate; 1-Amino-4-(tert-butoxycarbonyl)piperazine; 4-Aminopiperazine-1-carboxylicacid tert-butyl ester; tert-Butyl 4-aminopiperazine-1-carboxylate

Chemical Property of 1-TERT-BUTYLOXYCARBONYL-4-AMINO-PIPERAZINE

Chemical Property:

• Boiling Point: 281℃
• PKA: 7.03±0.20(Predicted)
• Flash Point: 124℃
• PSA: 58.80000
• Density: 1.097
• LogP: 0.98890
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl4-Aminopiperazine-1-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-TERT-BUTYLOXYCARBONYL-4-AMINO-PIPERAZINE

There total 6 articles about 1-TERT-BUTYLOXYCARBONYL-4-AMINO-PIPERAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl 4-nitrosopiperazine-1-carboxylate (877177-42-9) → 4-Amino-piperazine-1-carboxylic acid tert-butyl ester (118753-66-5)

Guidance literature:

tert-butyl 4-nitrosopiperazine-1-carboxylate; With acetic acid; zinc; In methanol; at 0 - 20 ℃; for 2h;

With sodium hydrogencarbonate; In methanol; water;

Reference yield:

4-nitropiperazine-1-carboxylic acid tert-butyl ester → 4-Amino-piperazine-1-carboxylic acid tert-butyl ester (118753-66-5)

Guidance literature:

With ammonium chloride; zinc; In tetrahydrofuran; water; for 0.5h;

Reference yield:

tert-butyl 4-carbamoylpiperazine-1-carboxylate (883554-88-9) → 4-Amino-piperazine-1-carboxylic acid tert-butyl ester (118753-66-5)

Guidance literature:

tert-butyl 4-carbamoylpiperazine-1-carboxylate; With sodium hypochlorite; sodium hydroxide; In ethanol; at 0 - 20 ℃;

With hydrogenchloride; In ethanol; water; at 20 ℃; for 0.25h; pH=~ 1;

With potassium carbonate; In ethanol; water;

upstream raw materials:

di-tert-butyl dicarbonate

piperazin-1-yl-amine

N-(tert-butyloxycarbonyl)bis(2-chloroethyl)amine

tert-butyl 4-nitrosopiperazine-1-carboxylate

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