iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

Base Information

Chemical Name:iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)
CAS No.:1393640-90-8
Molecular Formula:C₁₈H₂₉CuIN₂O₃Si
Molecular Weight:539.976
Hs Code.:

Synonyms:iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

Suppliers and Price of iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

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Technology Process of iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

There total 2 articles about iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1174062-52-2
1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

: 1393640-90-8
iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

Guidance literature:: With copper(l) iodide; sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1007/s10562-012-0880-7

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 1393640-90-8
iodo-1-mesityl-3-(3-trimethoxysilylpropyl)imidazol-2-ylidenecopper(I)

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; water / 16 h / 20 °C

1.2: 1 h / Reflux

1.3: 6 h / Reflux

2.1: 1,4-dioxane / 12 h / Inert atmosphere; Reflux

3.1: copper(l) iodide; sodium t-butanolate / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

With copper(l) iodide; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1007/s10562-012-0880-7