1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

Base Information

Chemical Name:1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide
CAS No.:1174062-52-2
Molecular Formula:C₁₈H₂₉N₂O₃Si*I
Molecular Weight:476.43
Hs Code.:

Synonyms:1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

Chemical Property:

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Technology Process of 1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

There total 4 articles about 1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 14867-28-8
3-iodopropyltrimethoxysilane

: 1174062-52-2
1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

Guidance literature:: In 1,4-dioxane; at 120 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c0dt00760a

Reference yield: 94.0%

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 2530-87-2
3-Chloropropyltrimethoxysilan

: 1174062-52-2
1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

Guidance literature:: With potassium iodide; In 1,2-dimethoxyethane; at 85 ℃; for 60h; Inert atmosphere;
DOI:10.1055/s-0028-1088053

Reference yield:

: 2530-87-2
3-Chloropropyltrimethoxysilan

: 1174062-52-2
1-[3-(trimethoxysilyl)propyl]-3-(2,4,6-trimethylphenyl)imidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 24 h / Inert atmosphere; Reflux

2: 1,4-dioxane / 12 h / 120 °C / Inert atmosphere

With sodium iodide; In 1,4-dioxane; acetone;
DOI:10.1039/c0dt00760a