C₁₄H₂₀BClO₃

Base Information

• Chemical Name: C₁₄H₂₀BClO₃
• CAS No.: 1310956-28-5
• Molecular Formula: C₁₄H₂₀BClO₃
• Molecular Weight: 282.575
• Mol file: 1310956-28-5.mol

Synonyms:C₁₄H₂₀BClO₃

Chemical Property of C₁₄H₂₀BClO₃

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀BClO₃

There total 2 articles about C₁₄H₂₀BClO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1-bromo-4-chloro-3-ethoxybenzene (900174-61-0) + bis(pinacol)diborane (73183-34-3) → C14H20BClO3 (1310956-28-5)

Guidance literature:

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; In 1,4-dioxane; at 90 ℃; for 5h;

Reference yield:

5-bromo-2-chlorophenol (183802-98-4) → C14H20BClO3 (1310956-28-5)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 70 °C

2: potassium acetate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 1,4-dioxane / 5 h / 90 °C

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; potassium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield: 19.0%

C14H20BClO3 (1310956-28-5) + C10H11BrN4O2 (882293-87-0) → C16H15ClN4O3 (1611446-03-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium carbonate; In 1,4-dioxane; at 100 ℃; for 17h;

upstream raw materials:

5-bromo-2-chlorophenol

1-bromo-4-chloro-3-ethoxybenzene

bis(pinacol)diborane

Downstream raw materials:

C₁₆H₁₅ClN₄O₃