(2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

Base Information

Chemical Name:(2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid
CAS No.:182075-77-0
Molecular Formula:C₂₃H₂₇NO₇
Molecular Weight:429.47
Hs Code.:

Synonyms:(2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

Suppliers and Price of (2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

Chemical Property:

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Technology Process of (2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

There total 4 articles about (2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 21768-33-2
(2S,3R)-2-amino-4-(benzyloxy)-3-hydroxybutanoic acid

: 104253-38-5
monobenzyl glutaryl N-hydroxysuccinimide

: 182075-77-0
(2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

Guidance literature:: With triethylamine; In water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)01114-8

Reference yield:

: 108-55-4
glutaric anhydride,

: 182075-77-0
(2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / DMAP / pyridine / 50 °C

2: 46 percent / CH₂Cl₂

3: 90 percent / Et₃N / dimethylformamide; H₂O

With dmap; triethylamine; In pyridine; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)01114-8

Reference yield:

: 54322-10-0
glutaric acid monobenzyl ester

: 182075-77-0
(2S,3R)-4-Benzyloxy-2-(4-benzyloxycarbonyl-butyrylamino)-3-hydroxy-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / CH₂Cl₂

2: 90 percent / Et₃N / dimethylformamide; H₂O

With triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)01114-8