2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

Base Information

Chemical Name:2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on
CAS No.:110372-72-0
Molecular Formula:C₂₈H₂₈O₅
Molecular Weight:444.527
Hs Code.:

Synonyms:2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

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Chemical Property of 2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

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Technology Process of 2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

There total 3 articles about 2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110372-68-4
2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

: 110372-72-0
2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

Guidance literature:: With sodium periodate; In water; acetone; at 50 ℃; for 4h;

Reference yield:

: 110372-63-9
1D-(1,2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsiloxy)methyl>-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

: 110372-72-0
2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DMSO, Ac₂O / 14 h / Ambient temperature

2: 80 percent / NaIO₄ / acetone; H₂O / 4 h / 50 °C

With sodium periodate; acetic anhydride; dimethyl sulfoxide; In water; acetone;

Reference yield:

: 107960-18-9,110453-99-1
(2S,3R,4S,5S)-2,3,4-Tris-benzyloxy-5-ethylsulfanyl-5-hydroxymethyl-cyclohexanol

: 110372-72-0
2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / pyridine / dimethylformamide / 1.) 0 deg C, 30 min 2.) RT, 9 h

2: 90 percent / DMSO, Ac₂O / 14 h / Ambient temperature

3: 80 percent / NaIO₄ / acetone; H₂O / 4 h / 50 °C

With pyridine; sodium periodate; acetic anhydride; dimethyl sulfoxide; In water; N,N-dimethyl-formamide; acetone;