1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol

Base Information

• Chemical Name: 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol
• CAS No.: 75348-19-5
• Molecular Formula: C₂₈H₃₀O₅
• Molecular Weight: 446.543

Synonyms:1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol

Chemical Property of 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol

Chemical Property:

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Technology Process of 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol

There total 29 articles about 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen (75348-18-4) → 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol (75348-19-5)

Guidance literature:

With sodium methylate; In methanol; Ambient temperature;

Reference yield: 84.0%

2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on (110372-72-0) → 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol (75348-19-5)

Guidance literature:

With hydrogenchloride; sodium cyanoborohydride; 3 A molecular sieve; In methanol;

Reference yield: 82.0%

(1R,2S,3S,4R)-1-O-benzoyl-5-(benzoyloxymethyl)-2,3,4-tri-O-benzyl-5-cyclohexene-1,2,3,4-tetrol (109923-15-1,109959-11-7) → 1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol (75348-19-5)

Guidance literature:

With sodium methylate; Ambient temperature;

DOI:10.1016/S0008-6215(00)90027-2

upstream raw materials:

2D-(2,4/3)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-2,3,4-trihydroxy-5-cyclohexen-1-on

1L-(1,3/2,4)-1-O-Acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-5-cyclohexen-1,2,3,4-tetrol

1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

(1R,2S,3S,4R)-1-O-benzoyl-5-(benzoyloxymethyl)-2,3,4-tri-O-benzyl-5-cyclohexene-1,2,3,4-tetrol

Downstream raw materials:

1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

(1R,2S,3S,4R)-2,3,4-tri-O-benzyl-5-(trityloxymethyl)-5-cyclohexene-1,2,3,4-tetrol

1L-(1,2,4/3,5)-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-2,3,4,5-cyclohexantetrol

1L-(1,3,5/2,4)-2,3,4-Tri-O-benzyl-5-C-hydroxymethyl-1,2,3,4-cyclohexantetrol

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