N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide

Base Information

• Chemical Name: N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide
• CAS No.: 420086-61-9
• Molecular Formula: C₁₆H₁₇BrClNO₃
• Molecular Weight: 386.673

Synonyms:N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide

Chemical Property of N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide

Chemical Property:

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Technology Process of N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide

There total 2 articles about N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroacetyl chloride (79-04-9) + (6-bromo-benzo[1,3]dioxol-5-ylmethyl)-cyclohexylidene-amine → N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide (420086-61-9)

Guidance literature:

With triethylamine; In toluene; at 20 ℃; for 3h;

DOI:10.1021/ol025534e

Reference yield:

1-bromo-6-aminomethyl-3,4-(methylenedioxy)-benzene (67496-29-1) → N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide (420086-61-9)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 3 h / Heating

2: Et₃N / toluene / 3 h / 20 °C

With triethylamine; In toluene;

DOI:10.1021/ol025534e

Reference yield: 95.0%

potassium ethyl xanthogenate (140-89-6) + N-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-2-chloro-N-cyclohex-1-enyl-acetamide (420086-61-9) → dithiocarbonic acid S-{[(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-cyclohex-1-enyl-carbamoyl]-methyl} ester O-ethyl ester (420086-62-0)

Guidance literature:

In acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/ol025534e

upstream raw materials:

chloroacetyl chloride

1-bromo-6-aminomethyl-3,4-(methylenedioxy)-benzene

Downstream raw materials:

dithiocarbonic acid S-{[(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-cyclohex-1-enyl-carbamoyl]-methyl} ester O-ethyl ester

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