tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

Base Information

Chemical Name:tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate
CAS No.:142535-09-9
Molecular Formula:C₃₂H₄₀N₂O₆
Molecular Weight:548.679
Hs Code.:

Synonyms:tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

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Chemical Property of tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

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Technology Process of tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

There total 4 articles about tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 142535-08-8
tert-butyl (E)-4-<<3-(2-carbomethoxyvinyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

: 142535-09-9
tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 1.5h; under 2585.7 Torr;
DOI:10.1021/jm00091a010

Reference yield:

: 104436-91-1
t-butyl 4-bromomethyl-3-methoxybenzoate

: 142535-09-9
tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 48 h

2: 90 percent / dioxane / 48 h / Heating

3: 92 percent / H₂ / 10percent Pd/C / methanol; tetrahydrofuran / 1.5 h / 2585.7 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00091a010

Reference yield:

: 142535-02-2
6-(cyclopentylacetamido)-3-formylindole

: 142535-09-9
tert-butyl 4-<<3-(2-carbomethoxyethyl)-6-(cyclopentylacetamido)indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 48 h

2: 90 percent / dioxane / 48 h / Heating

3: 92 percent / H₂ / 10percent Pd/C / methanol; tetrahydrofuran / 1.5 h / 2585.7 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00091a010