α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester

Base Information

Chemical Name:α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester
CAS No.:227007-19-4
Molecular Formula:C₂₂H₃₅N₃O₆
Molecular Weight:437.536
Hs Code.:

Synonyms:α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester

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Chemical Property of α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester

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Technology Process of α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester

There total 3 articles about α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53054-02-7
N_α-(1,1-dimethylethoxycarbonyl)-N_δ-(phenylmethoxycarbonyl)-L-ornithine 1,1-dimethylethyl ester

: 227007-19-4
α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10 percent Pd/C / methanol / 12 h / 3102.89 Torr

2: aq. Na₂CO₃ / CH₂Cl₂ / 1 h / 23 °C

3: CH₂Cl₂; methanol

With hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm980232x

Reference yield:

: 53054-03-8
tert-butyl (2S)-5-amino-2-[(2-methylpropan-2-yl)oxycarbonylamino]pentanoate

: 227007-19-4
α-N-tert-butoxycarbonyl-ω-N-hydroxy(O-benzyl)-L-citrulline tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. Na₂CO₃ / CH₂Cl₂ / 1 h / 23 °C

2: CH₂Cl₂; methanol

With sodium carbonate; In methanol; dichloromethane;
DOI:10.1021/jm980232x