Technology Process of C12H11ClN2O
There total 3 articles about C12H11ClN2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; potassium phosphate; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 29 h / 110 °C / Schlenk technique; Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 24 h / Inert atmosphere; Schlenk technique
With
potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/jo500064j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; potassium phosphate; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 29 h / 110 °C / Schlenk technique; Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 24 h / Inert atmosphere; Schlenk technique
With
potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/jo500064j
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 24h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jo500064j