methyl chloromethylbenzylcarbamate

Base Information

• Chemical Name: methyl chloromethylbenzylcarbamate
• CAS No.: 39074-40-3
• Molecular Formula: C₁₀H₁₂ClNO₂
• Molecular Weight: 213.664
• Mol file: 39074-40-3.mol

Synonyms:methyl chloromethylbenzylcarbamate

Chemical Property of methyl chloromethylbenzylcarbamate

Chemical Property:

Purity/Quality:

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Technology Process of methyl chloromethylbenzylcarbamate

There total 1 articles about methyl chloromethylbenzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + methyl N-benzylcarbamate (5817-70-9) → methyl chloromethylbenzylcarbamate (39074-40-3)

Guidance literature:

With chloro-trimethyl-silane; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ol100220c

Reference yield: 78.0%

methyl chloromethylbenzylcarbamate (39074-40-3) + 5-methylene-3,3a,4,5-tetrahydro-2H-pyrrolo[1,2-a]quinolin-1-one → C23H26N2O4 (1219744-16-7)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at 20 ℃; Cooling with ice; Inert atmosphere;

DOI:10.1021/ol100220c

upstream raw materials:

formaldehyd

methyl N-benzylcarbamate

Downstream raw materials:

C₂₃H₂₆N₂O₄