(1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate

Base Information

• Chemical Name: (1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate
• CAS No.: 1215294-92-0
• Molecular Formula: C₂₃H₃₈O₅SSi
• Molecular Weight: 454.703

Synonyms:(1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate

Chemical Property of (1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate

Chemical Property:

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Technology Process of (1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate

There total 1 articles about (1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(1R,2S,4S)-2-(3,4-dimethoxybenzylthio)-4-hydroxycyclohexyl acetate (1215294-90-8) + tert-butyldimethylsilyl chloride (18162-48-6) → (1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate (1215294-92-0)

Guidance literature:

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1039/b916506a

Reference yield: 95.0%

(1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexyl acetate (1215294-92-0) → (1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexanol (1215294-93-1)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 18h;

DOI:10.1039/b916506a

upstream raw materials:

(1R,2S,4S)-2-(3,4-dimethoxybenzylthio)-4-hydroxycyclohexyl acetate

tert-butyldimethylsilyl chloride

Downstream raw materials:

(1R,2S,4S)-4-(tert-butyldimethylsilyloxy)-2-(3,4-dimethoxybenzylthio)cyclohexanol

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