1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne

Base Information

• Chemical Name: 1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne
• CAS No.: 1162675-18-4
• Molecular Formula: C₆₈H₆₅N₂O₇P
• Molecular Weight: 1053.25

Synonyms:1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne

Chemical Property of 1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne

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Technology Process of 1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne

There total 1 articles about 1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-[3-({3-[4-(3-{[3-({2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}methyl)phenyl]ethynyl}phenyl)buta-1,3-diynyl]phenyl}ethynyl)benzyloxy]ethanol (1162675-14-0) + N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) → 1-{3-[(3-{2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}benzyloxy)ethynyl]phenyl}-4-{3-[(3-{2-[(2-cyanoethoxy)(diisopropyl)phosphinoxy]ethoxy}benzyloxy)ethynyl]phenyl}buta-1,3-diyne (1162675-18-4)

Guidance literature:

With N,N-diisopropylamine tetrazolide; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1002/hlca.200800397

upstream raw materials:

2-[3-({3-[4-(3-{[3-({2-[bis(4-methoxyphenyl)phenylmethoxy]ethoxy}methyl)phenyl]ethynyl}phenyl)buta-1,3-diynyl]phenyl}ethynyl)benzyloxy]ethanol

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

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