(2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

Base Information

Chemical Name:(2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate
CAS No.:114529-85-0
Molecular Formula:C₂₇H₃₇NO₃S
Molecular Weight:455.662
Hs Code.:

Synonyms:(2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

Suppliers and Price of (2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

There total 1 articles about (2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6258-60-2
p-methoxybenzylmercaptan

: trans-2-((-)-menthyloxycarbonyl)-3-phenylaziridine

: 114529-86-1
(2S,3R)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

: 114529-85-0
(2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1021/jo00249a006

Reference yield: 95.0%

: 68206-45-1
3-nitro-2-pyridinesulfenyl chloride

: 114529-85-0
(2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

: 114529-90-7
(2R,3S)-(-)-menthyl 2-amino-3-((S-3-nitro-2-pyridinesulfenyl)thio)-3-phenylpropionate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/jo00249a006

Reference yield:

: 114529-85-0
(2R,3S)-(-)-menthyl 2-amino-3-((4-methoxybenzyl)thio)-3-phenylpropionate

: (2R,3S)-2-Amino-3-(3-nitro-pyridin-2-yldisulfanyl)-3-phenyl-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CF₃COOH / CH₂Cl₂ / 0.25 h / 0 °C

2: aq. HF / 1 h / 0 °C

With hydrogen fluoride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo00249a006