1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

Base Information

Chemical Name:1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene
CAS No.:885058-74-2
Molecular Formula:C₁₆H₂₄I₂O₅
Molecular Weight:550.173
Hs Code.:

Synonyms:1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

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Technology Process of 1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

There total 1 articles about 1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 540-38-5
p-Iodophenol

: 76871-59-5
1,14-diiodo-3,6,9,12-tetraoxatetradecane

: 885058-74-2
1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

Guidance literature:: With potassium carbonate; In acetone; for 3h; Heating;
DOI:10.1021/ol060025o

Reference yield: 95.0%

: 885058-74-2
1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

: 33288-79-8
4,4'-dihydroxybenzil

: 885058-75-3
1,2-bis-(4-{2-[2-(2-{2-[2-(4-iodo-phenoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-phenyl)-ethane-1,2-dione

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1021/ol060025o

Reference yield:

: 885058-74-2
1-iodo-4-[2-(2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzene

: 885058-76-4
1,2-bis-[4-(2-{2-[2-(2-{2-[4-(4-methoxy-phenylethynyl)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-ethane-1,2-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Cs₂CO₃ / dimethylformamide / 80 °C

2: 80 percent / 1,3-bis(diphenylphosphino)propane; iPr₂NEt; CuI / palladium acetate / toluene / 16 h / 60 °C

With copper(l) iodide; 1,3-bis-(diphenylphosphino)propane; caesium carbonate; N-ethyl-N,N-diisopropylamine; palladium diacetate; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol060025o