2-Benzylbenzyl methanesulfonate

Base Information

Chemical Name:2-Benzylbenzyl methanesulfonate
CAS No.:1026077-03-1
Molecular Formula:C₁₅H₁₆O₃S
Molecular Weight:276.356
Hs Code.:

Synonyms:2-Benzylbenzyl methanesulfonate

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Chemical Property of 2-Benzylbenzyl methanesulfonate

Chemical Property:

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Technology Process of 2-Benzylbenzyl methanesulfonate

There total 1 articles about 2-Benzylbenzyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1586-00-1
2-(benzyl)benzyl alcohol

: 124-63-0
methanesulfonyl chloride

: 1026077-03-1
2-Benzylbenzyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jm00077a001

Reference yield:

: 1026077-03-1
2-Benzylbenzyl methanesulfonate

: 152495-39-1
5-Benzyl-2-diphenylacetyl-1,2,3,4-tetrahydro-isoquinoline-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) EtOH, 5 min, 2.) EtOH, RT, overnight

2: P₂O₅ / toluene / 4 h / Heating

3: NaCNBH₃ / acetic acid / 0.25 h / Ambient temperature

4: 1.) KOH, 2.) sulfuric acid / 1.) methanol, reflux, 4 h, 2.) reflux, 4 h

5: 1.) diisopropylethylamine / 1.) THF, 5 min, 2.) THF, RT, overnight

With potassium hydroxide; sulfuric acid; phosphorus pentoxide; sodium hydride; sodium cyanoborohydride; N-ethyl-N,N-diisopropylamine; In acetic acid; toluene;
DOI:10.1021/jm00077a001

Reference yield:

: 1026077-03-1
2-Benzylbenzyl methanesulfonate

: 152495-42-6,151888-46-9,151888-47-0
2-Diphenylacetyl-5-benzyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaH / 1.) EtOH, 5 min, 2.) EtOH, RT, overnight

2: P₂O₅ / toluene / 4 h / Heating

3: NaCNBH₃ / acetic acid / 0.25 h / Ambient temperature

4: 1.) KOH, 2.) sulfuric acid / 1.) methanol, reflux, 4 h, 2.) reflux, 4 h

5: 1.) diisopropylethylamine / 1.) THF, 5 min, 2.) THF, RT, overnight

6: 1.0 N aq. NaOH / methanol; tetrahydrofuran / 4 h

With potassium hydroxide; sodium hydroxide; sulfuric acid; phosphorus pentoxide; sodium hydride; sodium cyanoborohydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; acetic acid; toluene;
DOI:10.1021/jm00077a001