di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

Base Information

Chemical Name:di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine
CAS No.:97226-63-6
Molecular Formula:C₆₆H₉₉Cl₂N₁₅O₁₆P₂Si₄
Molecular Weight:1603.8
Hs Code.:

Synonyms:di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

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Chemical Property of di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

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Technology Process of di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

There total 1 articles about di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈₆H₁₁₅Cl₂N₁₅O₁₇P₂Si₄

: 97226-63-6
di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

Guidance literature:: With dichloro-acetic acid; In dichloromethane; at 25 ℃; for 2h; Yield given;
DOI:10.1016/S0040-4039(00)89130-3

Reference yield:

: 41662-41-3
bis(2,2,2-trichloroethyl) phosphorochloridite

: 97226-63-6
di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

: C₇₀H₁₀₂Cl₈N₁₅O₁₈P₃Si₄

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1016/S0040-4039(00)89130-3

Reference yield:

: 41662-41-3
bis(2,2,2-trichloroethyl) phosphorochloridite

: 97226-63-6
di-o-chlorophenyl 3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

: 97205-07-7
di-o-chlorophenyl 5'-O-bis(2,2,2-trichloroethyl)phosphoryl-3'-O-t-butyldimethylsilyladenylyl(2'-5')-3'-O-t-butyldimethylsilyladenylyl(2'-5')-2',3'-bis-O-(t-butyldimethylsilyl)adenosine

Guidance literature:: With 2,6-dimethylpyridine; iodine; sodium hydrogencarbonate; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) THF, ether, RT, 15 min;