5-methoxy-2-[3-(methylthio)propyl]aniline

Base Information

Chemical Name:5-methoxy-2-[3-(methylthio)propyl]aniline
CAS No.:1050514-06-1
Molecular Formula:C₁₁H₁₇NOS
Molecular Weight:211.328
Hs Code.:

Synonyms:5-methoxy-2-[3-(methylthio)propyl]aniline

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Chemical Property of 5-methoxy-2-[3-(methylthio)propyl]aniline

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Technology Process of 5-methoxy-2-[3-(methylthio)propyl]aniline

There total 7 articles about 5-methoxy-2-[3-(methylthio)propyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: (E)-4-methoxy-1-[3-(methylthio)prop-1-enyl]-2-nitrobenzene

: 1050514-06-1
5-methoxy-2-[3-(methylthio)propyl]aniline

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; for 12h; under 5149.01 Torr;

Reference yield:

: 17484-36-5
4-Methyl-3-nitroanisole

: 1050514-06-1
5-methoxy-2-[3-(methylthio)propyl]aniline

Guidance literature:: Multi-step reaction with 8 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 24 h / 80 °C

2: water; sodium hydrogencarbonate / 22 h / Heating / reflux

3: pyridine / piperidine / 12 h / 125 °C

4: thionyl chloride / 3 h / 0 °C / Heating / reflux

5: diisobutylaluminium hydride / toluene / 3 h / 0 - 20 °C

6: pyridine; bromine; triphenylphosphine / dichloromethane / 4 h / 0 - 20 °C

7: dichloromethane / 12 h / 20 °C

8: hydrogen / palladium 10% on activated carbon / ethanol / 12 h / 5149.01 Torr

With pyridine; N-Bromosuccinimide; thionyl chloride; water; hydrogen; bromine; diisobutylaluminium hydride; sodium hydrogencarbonate; triphenylphosphine; dibenzoyl peroxide; piperidine; palladium 10% on activated carbon; In tetrachloromethane; ethanol; dichloromethane; toluene;

Reference yield:

: 22996-21-0
4-methoxy-2-nitro-benzaldehyde

: 1050514-06-1
5-methoxy-2-[3-(methylthio)propyl]aniline

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / piperidine / 12 h / 125 °C

2: thionyl chloride / 3 h / 0 °C / Heating / reflux

3: diisobutylaluminium hydride / toluene / 3 h / 0 - 20 °C

4: pyridine; bromine; triphenylphosphine / dichloromethane / 4 h / 0 - 20 °C

5: dichloromethane / 12 h / 20 °C

6: hydrogen / palladium 10% on activated carbon / ethanol / 12 h / 5149.01 Torr

With pyridine; thionyl chloride; hydrogen; bromine; diisobutylaluminium hydride; triphenylphosphine; piperidine; palladium 10% on activated carbon; In ethanol; dichloromethane; toluene;