1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole

Base Information

• Chemical Name: 1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole
• CAS No.: 776317-25-0
• Molecular Formula: C₁₇H₁₉F₃N₂O
• Molecular Weight: 324.346

Synonyms:1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole

Chemical Property of 1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole

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Technology Process of 1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole

There total 1 articles about 1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-cyclobutyl-4-[(4-ethylphenyl)methyl]-5-trifluoromethyl-3-O-t-butyldimethylsilyl-1H-pyrazole (475149-33-8) → 1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole (776317-25-0)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; methanol; at 20 ℃;

Reference yield: 45.0%

1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole (776317-25-0) + 2,3,4,6-tetra-O-acetyl-5-thio-D-glucopyranose (137886-82-9) → 1'-cyclobutyl-4'-(4'-ethylbenzyl)-5'-trifluoromethyl-1'H-pyrazol-3'-yl 2,3,4,6-tetra-O-acetyl-5-thio-β-D-glucopyranoside

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 15h;

Reference yield:

1-cyclobutyl-4-[(4-ethylphenyl)methyl]-3-hydroxy-5-trifluoromethyl-1H-pyrazole (776317-25-0) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → 1'-cyclobutyl-4'-[(4-ethylphenyl)methyl]-5'-trifluoromethyl-1H-pyrazole-3'-O-(2,3,4,6-tetraacetyl)-β-D-glucopyranoside

Guidance literature:

With benzyltri(n-butyl)ammonium chloride; potassium carbonate; In chloroform; water; at 20 ℃; for 18h;

upstream raw materials:

1-cyclobutyl-4-[(4-ethylphenyl)methyl]-5-trifluoromethyl-3-O-t-butyldimethylsilyl-1H-pyrazole

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