N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Base Information

Chemical Name:N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine
CAS No.:479677-97-9
Molecular Formula:C₃₅H₅₄N₄O₅Si
Molecular Weight:638.923
Hs Code.:

Synonyms:N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Suppliers and Price of N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

There total 4 articles about N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5089-72-5
3-[N-(2-aminoethyl)]aminopropyltriethoxysilane

: 31795-93-4
N-benzyl-L-proline

: 479677-97-9
N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Guidance literature:: N-benzyl-L-proline; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 5 - 10 ℃; for 0.5h;

3-[N-(2-aminoethyl)]aminopropyltriethoxysilane; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1016/S0022-328X(02)01469-9

Reference yield:

: 5089-72-5
3-[N-(2-aminoethyl)]aminopropyltriethoxysilane

: 479677-97-9
N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; ethyl chloroformate / tetrahydrofuran / 0.5 h / 5 - 10 °C

1.2: 96 percent / tetrahydrofuran / 1 h / 0 °C

2.1: 98 percent / cyclohexene / Pd/C / ethanol / 1 h / Heating

3.1: triethylamine / tetrahydrofuran / 6 h / 0 °C

With chloroformic acid ethyl ester; triethylamine; cyclohexene; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-328X(02)01469-9

Reference yield:

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 479677-97-9
N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; ethyl chloroformate / tetrahydrofuran / 0.5 h / 5 - 10 °C

1.2: 96 percent / tetrahydrofuran / 1 h / 0 °C

2.1: 98 percent / cyclohexene / Pd/C / ethanol / 1 h / Heating

3.1: triethylamine / tetrahydrofuran / 6 h / 0 °C

With chloroformic acid ethyl ester; triethylamine; cyclohexene; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-328X(02)01469-9