(η-5-phenyltetramethylcyclopentadienyl)titanium trichloride

Base Information

Chemical Name:(η-5-phenyltetramethylcyclopentadienyl)titanium trichloride
CAS No.:166033-67-6
Molecular Formula:C₁₅H₁₇Cl₃Ti
Molecular Weight:351.539
Hs Code.:

Synonyms:(η-5-phenyltetramethylcyclopentadienyl)titanium trichloride

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Chemical Property of (η-5-phenyltetramethylcyclopentadienyl)titanium trichloride

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Technology Process of (η-5-phenyltetramethylcyclopentadienyl)titanium trichloride

There total 3 articles about (η-5-phenyltetramethylcyclopentadienyl)titanium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 166033-76-7
C₅(C₆H₅)(CH₃)4(Si(CH₃)3)

: 7550-45-0
titanium tetrachloride

: 166033-67-6
(η-5-phenyltetramethylcyclopentadienyl)titanium trichloride

Guidance literature:: In toluene; under Ar atm. using Schlenk techniques; recrystd. from toluene/pentane;
DOI:10.1021/om0109197

Reference yield: 46.0%

: Li(1-phenyl-2,3,4,5-tetramethylcyclopentadienyl)

: 7550-45-0
titanium tetrachloride

: 166033-67-6
(η-5-phenyltetramethylcyclopentadienyl)titanium trichloride

Guidance literature:: With SiMe₃Cl; In tetrahydrofuran; pentane; byproducts: LiCl; N2-atmosphere; refluxing cyclopentadienyl derivative with 1.5 equiv. SiClMe3 for 24 h, distn. off of THF, addn. of pentane, filtration off of LiCl, freezing, addn. of 0.9 equiv. TiCl4, slow warming to room temp., stirring for 10 h; crystn.; elem. anal.;
DOI:10.1016/S0022-328X(97)00327-6