tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

Base Information

Chemical Name:tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate
CAS No.:1027706-69-9
Molecular Formula:C₃₀H₃₆FN₃O₂S
Molecular Weight:521.699
Hs Code.:

Synonyms:tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

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Chemical Property of tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

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Technology Process of tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

There total 1 articles about tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027702-88-0
tert-butyl {[4-(3-fluorophenyl)piperidin-3-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

: 532-55-8
Benzoyl isothiocyanate

: 1027706-69-9
tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

Guidance literature:: tert-butyl {[4-(3-fluorophenyl)piperidin-3-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate; Benzoyl isothiocyanate; In toluene; at 20 ℃; for 2h;

With methylamine; In methanol; at 20 ℃; for 48h;

Reference yield:

: 1027706-69-9
tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

: 33142-21-1
ethyl 2-chloro-3-oxopropanoate

: 1027706-89-3
ethyl 2-[4-({(tert-butoxycarbonyl)[(1R)-1-(1-naphthyl)ethyl]amino}methyl)-3-(3-fluorophenyl)piperidin-1-yl]-1,3-thiazole-5-carboxylate

Guidance literature:: With magnesium sulfate; In acetone; benzene; at 65 ℃; for 4h;

Reference yield:

: 70-23-5
ethyl Bromopyruvate

: 1027706-69-9
tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate

: 1027706-76-8
2-[4-({(tert-butoxycarbonyl)[(1R)-1-(1-naphthyl)ethyl]amino}methyl)-3-(3-fluorophenyl)piperidin-1-yl]-1,3-thiazole-4-carboxylic acid

Guidance literature:: ethyl Bromopyruvate; tert-butyl {[1-(aminocarbonothioyl)-3-(3-fluorophenyl)piperidin-4-yl]methyl}[(1R)-1-(1-naphthyl)ethyl]carbamate; With sodium hydroxide; water; In ethanol; at 20 - 85 ℃; for 3h;

With hydrogenchloride; In water;