1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

Base Information

Chemical Name:1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one
CAS No.:1027141-42-9
Molecular Formula:C₂₉H₃₄O₆
Molecular Weight:478.585
Hs Code.:

Synonyms:1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

Suppliers and Price of 1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

There total 5 articles about 1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1026626-27-6
1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)octane-1,8-dione

: 1027141-42-9
1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In ethanol; for 0.5h; Ambient temperature;
DOI:10.1039/P29960001131

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1027141-42-9
1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 1.) Et₂O, 2.) Et₂O, benzene, reflux, 2 h

2: 90 percent / MnO₂ / acetone / 4 h / Ambient temperature

3: 33 percent / H₂ / 5percent Pd-C / tetrahydrofuran / 0.12 h / 760 Torr

4: 91 percent / NaBH₄, aq. NaOH / ethanol / 0.5 h / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; sodium tetrahydroborate; hydrogen; magnesium; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetone;
DOI:10.1039/P29960001131

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1027141-42-9
1-(4-hydroxy-3-methoxyphenyl)-8-(4-benzyloxy-3-methoxyphenyl)-8-hydroxyoctan-1-one

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / K₂CO₃ / acetone / 6 h / Heating

2: 1.) Mg / 1.) Et₂O, 2.) Et₂O, benzene, reflux, 2 h

3: 90 percent / MnO₂ / acetone / 4 h / Ambient temperature

4: 33 percent / H₂ / 5percent Pd-C / tetrahydrofuran / 0.12 h / 760 Torr

5: 91 percent / NaBH₄, aq. NaOH / ethanol / 0.5 h / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; sodium tetrahydroborate; hydrogen; potassium carbonate; magnesium; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetone;
DOI:10.1039/P29960001131