Technology Process of 3-oxo-5β-androstan-17α-yl cyclohexanecarboxylate
There total 7 articles about 3-oxo-5β-androstan-17α-yl cyclohexanecarboxylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 99 percent / NaBH4 / methanol; ethyl acetate; CH2Cl2 / 1 h
2: pyridine / 72 h / 30 °C
3: 44 percent / NaNO2 / dimethylsulfoxide / 1 h / 135 °C
4: 64 percent / pyridine / 20 h / Ambient temperature
5: 90 percent / conc. HCl / CHCl3; methanol / 64 h / Ambient temperature
6: 25 percent / H2 / Adams platinum catalyst / acetic acid / 2 h / Ambient temperature
7: 88 percent / Jones reagent / acetone
With
pyridine; hydrogenchloride; sodium tetrahydroborate; jones reagent; hydrogen; sodium nitrite;
platinum(IV) oxide;
In
methanol; dichloromethane; chloroform; acetic acid; dimethyl sulfoxide; ethyl acetate; acetone;
DOI:10.1135/cccc19930600
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 44 percent / NaNO2 / dimethylsulfoxide / 1 h / 135 °C
2: 64 percent / pyridine / 20 h / Ambient temperature
3: 90 percent / conc. HCl / CHCl3; methanol / 64 h / Ambient temperature
4: 25 percent / H2 / Adams platinum catalyst / acetic acid / 2 h / Ambient temperature
5: 88 percent / Jones reagent / acetone
With
pyridine; hydrogenchloride; jones reagent; hydrogen; sodium nitrite;
platinum(IV) oxide;
In
methanol; chloroform; acetic acid; dimethyl sulfoxide; acetone;
DOI:10.1135/cccc19930600
![Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester](/Databaselist/images/loading.webp)
