Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

Base Information

Chemical Name:Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester
CAS No.:150054-84-5
Molecular Formula:C₂₆H₄₂O₃
Molecular Weight:402.618
Hs Code.:

Synonyms:Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

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Chemical Property of Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

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Technology Process of Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

There total 6 articles about Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 40768-04-5
3β-hydroxyandrost-5-en-17α-yl benzoate

: 150054-83-4
3β-hydroxy-5α-androstan-17α-yl cyclohexanecarboxylate

: 150054-84-5
Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

Guidance literature:: With hydrogen; platinum(IV) oxide; In acetic acid; for 2h; Ambient temperature;
DOI:10.1135/cccc19930600

Reference yield:

: 853-23-6
prasterone acetate

: 150054-84-5
Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / NaBH₄ / methanol; ethyl acetate; CH₂Cl₂ / 1 h

2: pyridine / 72 h / 30 °C

3: 44 percent / NaNO₂ / dimethylsulfoxide / 1 h / 135 °C

4: 64 percent / pyridine / 20 h / Ambient temperature

5: 90 percent / conc. HCl / CHCl₃; methanol / 64 h / Ambient temperature

6: 25 percent / H₂ / Adams platinum catalyst / acetic acid / 2 h / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; hydrogen; sodium nitrite; platinum(IV) oxide; In methanol; dichloromethane; chloroform; acetic acid; dimethyl sulfoxide; ethyl acetate;
DOI:10.1135/cccc19930600

Reference yield:

: 1259-22-9
5-androstene-3β,17β-diol 3-acetate 17-p-toluene-δ-sulfonate

: 150054-84-5
Cyclohexanecarboxylic acid (3S,5R,8R,9S,10S,13S,14S,17R)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / NaNO₂ / dimethylsulfoxide / 1 h / 135 °C

2: 64 percent / pyridine / 20 h / Ambient temperature

3: 90 percent / conc. HCl / CHCl₃; methanol / 64 h / Ambient temperature

4: 25 percent / H₂ / Adams platinum catalyst / acetic acid / 2 h / Ambient temperature

With pyridine; hydrogenchloride; hydrogen; sodium nitrite; platinum(IV) oxide; In methanol; chloroform; acetic acid; dimethyl sulfoxide;
DOI:10.1135/cccc19930600