(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

Base Information

Chemical Name:(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one
CAS No.:869347-51-3
Molecular Formula:C₂₁H₁₈BrNO₂
Molecular Weight:396.283
Hs Code.:

Synonyms:(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

Suppliers and Price of (+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

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Chemical Property of (+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

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Technology Process of (+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

There total 1 articles about (+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 252010-35-8
(+/-)-6-ethyl-6-(p-tolyl)pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

: 869347-51-3
(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

Guidance literature:: With N-Bromosuccinimide; azobisisobutyronitrile; In tetrachloromethane; for 4h; Heating;
DOI:10.1021/jm050257d

Reference yield: 85.0%

: 869347-51-3
(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

: 169685-29-4
4-trifluoromethoxybenzenethiol

: 1268473-09-1
(+/-)-6-ethyl-6-[4-[(4-trifluoromethoxyphenylthio)methyl]-phenyl]-6,7-dihydrobenzo[b]pyrrolo[1,2-d][1,4]oxazepin-7-one

Guidance literature:: 4-trifluoromethoxybenzenethiol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 2h; Inert atmosphere;

(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one; In tetrahydrofuran; mineral oil; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jm101438u

Reference yield: 78.0%

: 869347-51-3
(+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one

: 100-52-7
benzaldehyde

: 5-ethyl-5-(4-styryl-phenyl)-6-oxa-10b-aza-benzo[e]azulen-4-one

Guidance literature:: (+/-)-6-ethyl-6-[4-(bromomethyl)phenyl]pyrrolo[2,1-d][1,5]benzoxazepin-7(6H)-one; With triethyl phosphite; for 2h; Heating;

With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

benzaldehyde; In tetrahydrofuran; at 60 ℃; for 5h;
DOI:10.1021/jm050257d