ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

Base Information

Chemical Name:ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt
CAS No.:1300724-22-4
Molecular Formula:C₃H₄N₂*C₁₁H₁₀Cl₂O₃
Molecular Weight:329.183
Hs Code.:

Synonyms:ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

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Chemical Property of ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

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Technology Process of ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

There total 1 articles about ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 6148-64-7
ethyl potassium malonate

: 530-62-1
1,1'-carbonyldiimidazole

: 1300724-22-4
ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

Guidance literature:: 2,4 dichlorobenzoic acid; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Industry scale;

ethyl potassium malonate; With magnesium chloride; In N,N-dimethyl-formamide; at 100 ℃; Industry scale;

Reference yield:

: 1300724-22-4
ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

: 62005-48-5
N-acetylaminoacetaldehyde dimethyl acetal

: 1300724-25-7
ethyl 2-(2,4-dichlorophenyl)-1H-pyrrole-3-carboxylate

Guidance literature:: ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt; N-acetylaminoacetaldehyde dimethyl acetal; With trifluoroacetic acid; at 60 ℃; for 1h;

With sodium hydrogencarbonate; In ethyl acetate;

With sodium hydroxide; In ethanol; at 20 ℃;

Reference yield:

: 1300724-22-4
ethyl 3-(2,4-dichlorophenyl)-3-oxopropanoate imidazole salt

: 5-(2-amino-pyrimidin-4-yl)-2-(2,4-dichloro-phenyl)-1H-pyrrole-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / 1 h / 60 °C

1.3: 20 °C

2.1: aluminum (III) chloride / dichloromethane / 0.5 h / 20 °C

3.1: 1,4-dioxane / 12 h / 95 °C

4.1: sodium ethanolate / ethanol / 24 h / Reflux

With sodium ethanolate; trifluoroacetic acid; aluminum (III) chloride; In 1,4-dioxane; ethanol; dichloromethane;