4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

Base Information

Chemical Name:4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid
CAS No.:1287220-85-2
Molecular Formula:C₂₃H₂₃F₃N₈O₅
Molecular Weight:548.481
Hs Code.:

Synonyms:4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

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Chemical Property of 4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

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Technology Process of 4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

There total 5 articles about 4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1287220-84-1
tert-butyl 4-(4-(4-(2-(2-(tert-butoxycarbonylamino)acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoate

: 1287220-85-2
4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 1h;

Reference yield:

: 18144-47-3
tert-butyl 4-aminobenzoate

: 1287220-85-2
4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 65 °C

3: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 16 h

4: hydrogenchloride / 1,4-dioxane / 1 h

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 185677-00-3
2,4-dichloro-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine

: 1287220-85-2
4-(4-(4-(2-(2-amino acetamido)acetamido)benzylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 65 °C

3: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 16 h

4: hydrogenchloride / 1,4-dioxane / 1 h

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; 1,4-dioxane; dichloromethane;