C₅₅H₅₉N₃O₁₀

Base Information

• Chemical Name: C₅₅H₅₉N₃O₁₀
• CAS No.: 566199-71-1
• Molecular Formula: C₅₅H₅₉N₃O₁₀
• Molecular Weight: 922.088
• Mol file: 566199-71-1.mol

Synonyms:C₅₅H₅₉N₃O₁₀

Chemical Property of C₅₅H₅₉N₃O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₅₉N₃O₁₀

There total 7 articles about C₅₅H₅₉N₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(2R,3R,4R,5S,6R)-2-((2R,3S,4S,5R,6R)-6-Azido-4,5-bis-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-ol (566199-62-0) + methyl iodide (74-88-4) → C55H59N3O10 (566199-71-1)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(03)00475-1

Reference yield:

1-amido-1-deoxygalactopyranose (35899-89-9) → C55H59N3O10 (566199-71-1)

Guidance literature:

Multi-step reaction with 8 steps

1: 95 percent / p-toluenesulfonic acid / acetonitrile

2: 86 percent / pyridine

3: 93 percent / sodium cyanoborohydride; HCl; MS AW-300 / tetrahydrofuran; diethyl ether / 4 h / 0 °C / pH 2

4: 67 percent / N-iodosuccinimide; trimethylsilyl trifluoromethanesulfonate; MS-AW₃₀₀ / CH₂Cl₂; diethyl ether / -50 °C

5: sodium methoxide; methanol / CH₂Cl₂

6: sodium hydride / dimethylformamide

7: 95 percent / trifluoroaceic acid / CH₂Cl₂ / 0 °C

8: 90 percent / sodium hydride / dimethylformamide

With pyridine; hydrogenchloride; methanol; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; MS AW-300; MS-AW₃₀₀; sodium methylate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1016/S0040-4039(03)00475-1

Reference yield:

benzaldehyde dimethyl acetal (1125-88-8) → C55H59N3O10 (566199-71-1)

Guidance literature:

Multi-step reaction with 8 steps

1: 95 percent / p-toluenesulfonic acid / acetonitrile

2: 86 percent / pyridine

3: 93 percent / sodium cyanoborohydride; HCl; MS AW-300 / tetrahydrofuran; diethyl ether / 4 h / 0 °C / pH 2

4: 67 percent / N-iodosuccinimide; trimethylsilyl trifluoromethanesulfonate; MS-AW₃₀₀ / CH₂Cl₂; diethyl ether / -50 °C

5: sodium methoxide; methanol / CH₂Cl₂

6: sodium hydride / dimethylformamide

7: 95 percent / trifluoroaceic acid / CH₂Cl₂ / 0 °C

8: 90 percent / sodium hydride / dimethylformamide

With pyridine; hydrogenchloride; methanol; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; MS AW-300; MS-AW₃₀₀; sodium methylate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1016/S0040-4039(03)00475-1

upstream raw materials:

(2R,3R,4R,5S,6R)-2-((2R,3S,4S,5R,6R)-6-Azido-4,5-bis-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-ol

methyl iodide

1-amido-1-deoxygalactopyranose

benzaldehyde dimethyl acetal