3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone

Base Information

• Chemical Name: 3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone
• CAS No.: 946528-69-4
• Molecular Formula: C₂₉H₃₈O₆
• Molecular Weight: 482.617
• Mol file: 946528-69-4.mol

Synonyms:3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone

Chemical Property of 3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone

There total 2 articles about 3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(C6H6O3CCH2C7H12)2 → 3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone (946528-69-4)

Guidance literature:

With tin(IV) oxide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ol070951i

Reference yield:

2-cyclohexylmethyl-3,4-dimethoxyphenol (180912-48-5) → 3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone (946528-69-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N; Ag₂O / CHCl₃ / 1 h / 20 °C

2: 26.6 mg / SnO₂ / CH₂Cl₂ / 1 h / 20 °C

With tin(IV) oxide; triethylamine; silver(l) oxide; In dichloromethane; chloroform;

DOI:10.1021/ol070951i

Reference yield: 94.0%

3-(cyclohexylmethyl)-5-(3'-cyclohexylmethyl-2'-hydroxy-4',5'-dimethoxyphenyl)-2-methoxy-[1,4]benzoquinone (946528-69-4) → 2,6-bis(cyclohexylmethyl)-3,7,8-trimethoxydibenzofuran-1,4-dione (180912-63-4)

Guidance literature:

With oxygen; chloranil; In toluene; at 100 ℃; for 96h;

DOI:10.1021/ol070951i

upstream raw materials:

2-cyclohexylmethyl-3,4-dimethoxyphenol

Downstream raw materials:

2,6-bis(cyclohexylmethyl)-3,7,8-trimethoxydibenzofuran-1,4-dione