(19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

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Chemical Name:(19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate
CAS No.:1228927-28-3
Molecular Formula:C₂₇H₄₇N₃O₆
Molecular Weight:509.687
Hs Code.:

(19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

Synonyms:(19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

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Chemical Property of (19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

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Technology Process of (19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

There total 2 articles about (19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 2432-99-7,25587-80-8,84029-94-7
11-aminoundecanoic acid

: 7633-32-1
tert-butyl glyoxylate

: 10111-08-7
2-imidazolecarbaldehyde

: 1228927-28-3
(19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

Guidance literature:: 11-aminoundecanoic acid; 2-imidazolecarbaldehyde; With acetic acid; In 1,2-dichloro-ethane; for 0.5h; Reflux;

tert-butyl glyoxylate; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 0 - 20 ℃;

Reference yield:

: 2432-99-7,25587-80-8,84029-94-7
11-aminoundecanoic acid

: 7633-32-1
tert-butyl glyoxylate

: 1226869-60-8
tert-butyl 2-(2-formyl-1H-imidazol-1-yl)acetate

: 1228927-28-3
(19S,23S)-tetra-tert-butyl-2-((1-(2-tertbutoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)-13,21-dioxo-2,14,20,22-tetraazapentacosane-1,19,23,25-tetracarboxylate

Guidance literature:: 11-aminoundecanoic acid; tert-butyl glyoxylate; tert-butyl 2-(2-formyl-1H-imidazol-1-yl)acetate; With acetic acid; In 1,2-dichloro-ethane; for 0.5h; Reflux; Inert atmosphere;

With sodium triacetoxyborohydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.ica.2012.03.002