ethyltriphenylphosphonium pentachloridooxidorhenate(VI)

Base Information

• Chemical Name: ethyltriphenylphosphonium pentachloridooxidorhenate(VI)
• CAS No.: 1166850-60-7
• Molecular Formula: C₂₀H₂₀P*Cl₅ORe
• Molecular Weight: 670.824
• Mol file: 1166850-60-7.mol

Synonyms:ethyltriphenylphosphonium pentachloridooxidorhenate(VI)

Chemical Property of ethyltriphenylphosphonium pentachloridooxidorhenate(VI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyltriphenylphosphonium pentachloridooxidorhenate(VI)

There total 1 articles about ethyltriphenylphosphonium pentachloridooxidorhenate(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + ethyltriphenylphosphonium rhenate(VII) → ethyltriphenylphosphonium pentachloridooxidorhenate(VI) (1166850-60-7)

Guidance literature:

In ethanol; byproducts: Cl2, H2O; HCl bubbled through a suspn. of Re compd., Re compd. added under HCl, sealed; crystd. for a few days at ca -10°C, filtered off;

DOI:10.1016/j.ica.2009.01.035

Reference yield:

ethyltriphenylphosphonium pentachloridooxidorhenate(VI) (1166850-60-7) + water (7732-18-5) → Cl4H2O2Re(1-)*C20H20P(1+)

Guidance literature:

With air; for 0.25h;

DOI:10.1016/j.ica.2014.04.041

upstream raw materials:

hydrogenchloride