Technology Process of 2-[4-(3,5-dichlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide
There total 2 articles about 2-[4-(3,5-dichlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: neat (no solvent) / 0.17 h / 185 °C / Microwave irradiation; Sealed tube
2.1: potassium carbonate / acetone / 0.08 h / 90 °C / Microwave irradiation; Sealed tube
2.2: 0.17 h / 90 °C / Microwave irradiation; Sealed tube
3.1: hydrazine hydrate / ethanol / 0.17 h / 130 °C / Microwave irradiation; Sealed tube
With
potassium carbonate; hydrazine hydrate;
In
ethanol; acetone;
DOI:10.3184/174751912X13400138806685
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / acetone / 0.08 h / 90 °C / Microwave irradiation; Sealed tube
1.2: 0.17 h / 90 °C / Microwave irradiation; Sealed tube
2.1: hydrazine hydrate / ethanol / 0.17 h / 130 °C / Microwave irradiation; Sealed tube
With
potassium carbonate; hydrazine hydrate;
In
ethanol; acetone;
DOI:10.3184/174751912X13400138806685
- Guidance literature:
-
2-[4-(3,5-dichlorophenyl)-3-methyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide;
With
potassium hydroxide;
In
ethanol; water;
at 100 ℃;
for 0.0833333h;
Microwave irradiation;
carbon disulfide;
In
ethanol; water;
at 100 ℃;
for 0.166667h;
Temperature;
Time;
Microwave irradiation;
DOI:10.3184/174751912X13400138806685
