1'-Benzylspiroimidazolin>-5'-on

Base Information

• Chemical Name: 1'-Benzylspiroimidazolin>-5'-on
• CAS No.: 78274-16-5
• Molecular Formula: C₁₂H₁₂N₂O
• Molecular Weight: 200.24

Synonyms:1'-Benzylspiroimidazolin>-5'-on

Chemical Property of 1'-Benzylspiroimidazolin>-5'-on

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Technology Process of 1'-Benzylspiroimidazolin>-5'-on

There total 2 articles about 1'-Benzylspiroimidazolin>-5'-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

methyl 1-isocyano cyclopropane carboxylate (71015-23-1) + benzylamine (100-46-9) → 1'-Benzylspiroimidazolin>-5'-on (78274-16-5)

Guidance literature:

With silver nitrate; In toluene; at 60 ℃; Inert atmosphere;

DOI:10.1021/acs.orglett.7b02334

Reference yield: 60.0%

1-Isocyan-1-cyclopropancarbonsaeure-ethylester (32755-45-6) + benzylamine (100-46-9) → 1'-Benzylspiroimidazolin>-5'-on (78274-16-5)

Guidance literature:

With toluene-4-sulfonic acid; for 1h;

upstream raw materials:

1-Isocyan-1-cyclopropancarbonsaeure-ethylester

benzylamine

methyl 1-isocyano cyclopropane carboxylate

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