3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

Base Information

Chemical Name:3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine
CAS No.:1145786-47-5
Molecular Formula:C₁₅H₁₃ClN₄O
Molecular Weight:300.747
Hs Code.:

Synonyms:3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

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Chemical Property of 3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

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Technology Process of 3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

There total 3 articles about 3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 791642-68-7
4-bromo-1-iodo-2-methoxybenzene

: 1145786-47-5
3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 8-quinolinol; copper(l) iodide; caesium carbonate

2.1: n-butyllithium; Triisopropyl borate

2.2: Reflux

With copper(l) iodide; 8-quinolinol; n-butyllithium; Triisopropyl borate; caesium carbonate; 2.2: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.04.143

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1145786-47-5
3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide

2.1: toluene-4-sulfonic acid; potassium iodide; sodium nitrite

3.1: 8-quinolinol; copper(l) iodide; caesium carbonate

4.1: n-butyllithium; Triisopropyl borate

4.2: Reflux

With N-Bromosuccinimide; copper(l) iodide; 8-quinolinol; n-butyllithium; Triisopropyl borate; caesium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; 4.2: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.04.143

Reference yield:

: 59557-91-4
4-bromo-2-methoxyaniline

: 1145786-47-5
3-chloro-6-[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid; potassium iodide; sodium nitrite

2.1: 8-quinolinol; copper(l) iodide; caesium carbonate

3.1: n-butyllithium; Triisopropyl borate

3.2: Reflux

With copper(l) iodide; 8-quinolinol; n-butyllithium; Triisopropyl borate; caesium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; 3.2: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.04.143