C₆₁H₁₀₈O₁₁Si₃

Base Information

Chemical Name:C₆₁H₁₀₈O₁₁Si₃
CAS No.:218785-37-6
Molecular Formula:C₆₁H₁₀₈O₁₁Si₃
Molecular Weight:1101.78
Hs Code.:

C<sub>61</sub>H<sub>108</sub>O<sub>11</sub>Si<sub>3</sub>

Synonyms:C₆₁H₁₀₈O₁₁Si₃

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Chemical Property of C₆₁H₁₀₈O₁₁Si₃

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Technology Process of C₆₁H₁₀₈O₁₁Si₃

There total 32 articles about C₆₁H₁₀₈O₁₁Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 218785-16-1
(4S,5S)-4-((S)-2-Bromo-1-methyl-allyl)-2,2,5-trimethyl-[1,3]dioxane

: 218785-37-6
C₆₁H₁₀₈O₁₁Si₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: t-BuLi / diethyl ether / 0.5 h / -78 - 0 °C

1.2: lithium 2-thienylcyanocuprate / 0.5 h / -78 - -45 °C

1.3: 83 percent / 48 h / -5 °C

2.1: 96 percent / KHMDS

3.1: OsO₄; NMO

3.2: 87 percent / NaIO₄

4.1: 84 percent / DIBAL

5.1: 51 percent / HO(CH₂)3OH; PPTS / tetrahydrofuran

6.1: pyridine

7.1: 2,6-lutidine

With pyridine; 2,6-dimethylpyridine; osmium(VIII) oxide; N-methyl-2-indolinone; tert.-butyl lithium; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; diisobutylaluminium hydride; trimethyleneglycol; In tetrahydrofuran; diethyl ether; 1.1: Metallation / 1.2: Addition / 1.3: coupling / 2.1: Methylation / 3.1: Oxidation / 3.2: cleavage / 4.1: Reduction / 5.1: deprotection / 6.1: Acylation / 7.1: silylation;
DOI:10.1021/ja992134m

Reference yield:

: 218785-25-2
Trifluoro-methanesulfonic acid (S)-1-methylene-2-((4S,5S)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-propyl ester

: 218785-37-6
C₆₁H₁₀₈O₁₁Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: (Bu₃Sn)2; n-BuLi; lithium 2-thienylcyanocuprate

1.2: NBS

2.1: t-BuLi / diethyl ether / 0.5 h / -78 - 0 °C

2.2: lithium 2-thienylcyanocuprate / 0.5 h / -78 - -45 °C

2.3: 83 percent / 48 h / -5 °C

3.1: 96 percent / KHMDS

4.1: OsO₄; NMO

4.2: 87 percent / NaIO₄

5.1: 84 percent / DIBAL

6.1: 51 percent / HO(CH₂)3OH; PPTS / tetrahydrofuran

7.1: pyridine

8.1: 2,6-lutidine

With pyridine; 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; tert.-butyl lithium; bis(tri-n-butyltin); pyridinium p-toluenesulfonate; potassium hexamethylsilazane; diisobutylaluminium hydride; thien-2-yl(cyano)copper lithium; trimethyleneglycol; In tetrahydrofuran; diethyl ether; 1.1: Substitution / 1.2: Substitution / 2.1: Metallation / 2.2: Addition / 2.3: coupling / 3.1: Methylation / 4.1: Oxidation / 4.2: cleavage / 5.1: Reduction / 6.1: deprotection / 7.1: Acylation / 8.1: silylation;
DOI:10.1021/ja992134m

Reference yield:

: 218785-05-8
[(2R,3S,5S,7R,8S,9S)-7-(2-Benzyloxy-ethyl)-3-(4-methoxy-benzyloxy)-4,4,8-trimethyl-2-(R)-oxiranyl-1,6-dioxa-spiro[4.5]dec-9-yloxy]-tert-butyl-dimethyl-silane

: 218785-37-6
C₆₁H₁₀₈O₁₁Si₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: t-BuLi / diethyl ether / 0.5 h / -78 - 0 °C

1.2: lithium 2-thienylcyanocuprate / 0.5 h / -78 - -45 °C

1.3: 83 percent / 48 h / -5 °C

2.1: 96 percent / KHMDS

3.1: OsO₄; NMO

3.2: 87 percent / NaIO₄

4.1: 84 percent / DIBAL

5.1: 51 percent / HO(CH₂)3OH; PPTS / tetrahydrofuran

6.1: pyridine

7.1: 2,6-lutidine

With pyridine; 2,6-dimethylpyridine; osmium(VIII) oxide; N-methyl-2-indolinone; tert.-butyl lithium; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; diisobutylaluminium hydride; trimethyleneglycol; In tetrahydrofuran; diethyl ether; 1.1: Metallation / 1.2: Addition / 1.3: coupling / 2.1: Methylation / 3.1: Oxidation / 3.2: cleavage / 4.1: Reduction / 5.1: deprotection / 6.1: Acylation / 7.1: silylation;
DOI:10.1021/ja992134m