Technology Process of C29H34O5
There total 7 articles about C29H34O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
vinylmagnesium chloride;
With
copper(I) bromide dimethylsulfide complex;
In
tetrahydrofuran; diethyl ether;
C27H30O5;
In
tetrahydrofuran; diethyl ether;
at -30 - 0 ℃;
for 12h;
With
ammonium chloride;
In
tetrahydrofuran; diethyl ether;
stereoselective reaction;
DOI:10.1016/j.tet.2011.10.024
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 21 °C
2.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / decane; dichloromethane / Molecular sieve
3.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran; diethyl ether
3.2: 12 h / -30 - 0 °C
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; copper(I) bromide dimethylsulfide complex; L-(+)-diisopropyl tartrate; diisobutylaluminium hydride;
In
tetrahydrofuran; diethyl ether; decane; hexane; dichloromethane;
2.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2011.10.024
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / decane; dichloromethane / Molecular sieve
2.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran; diethyl ether
2.2: 12 h / -30 - 0 °C
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; copper(I) bromide dimethylsulfide complex; L-(+)-diisopropyl tartrate;
In
tetrahydrofuran; diethyl ether; decane; dichloromethane;
1.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2011.10.024
